退火温度对依据LSDR原理轧制的Mg/Al层合板界面结构的影响

    Effect of Annealing Temperature on Interface structure of Mg/Al Laminated Composites Rolled under LSDR Principle

    • 摘要: 基于点阵强变形轧制(lattice severe deformation rolling,LSDR)原理制备了Mg/Al层合板,研究了200~400℃退火温度下界面扩散层厚度、成分以及形态特征,并进行了拉伸试验。结果表明:随退火温度升高,扩散层厚度逐渐增大。当退火温度为300℃时,界面由明显的两层组成,靠近镁合金一侧为Mg17Al12相,靠近铝合金一侧为Mg2Al3相,且随温度升高,Mg2Al3相比Mg17Al12相生长速度快;界面沿轧向(rolling direction,RD)和横向(transverse direction,TD)均连续分布。Mg/Al层合板沿RD和TD的抗拉强度以及伸长率随退火温度升高均呈先增大后减小规律,300℃退火时获得最优的力学性能,沿RD和TD抗拉强度最大值分别为242 MPa和247 MPa,同时伸长率超过14%,相较未经退火的板材有显著提高。研究结果为探究LSDR原理制备高质量Mg/Al层合板提供了试验参考。

       

      Abstract: Mg/Al laminated composites were prepared based on lattice severe deformation rolling(LSDR) principle.The thickness,composition and morphological characteristics of the interfacial layer were studied at 200℃-400℃annealing temperatures,and tensile tests were carried out.The results show that the thickness of diffusion layer increases with the increase of annealing temperature.When the annealing temperature reaches 300℃,the interface is composed of two layers,including Mg17Al12 phase near the magnesium alloy side and Mg2Al3 phase near the aluminum alloy side,and the growth rate of Mg2Al3 phase is faster than that of Mg17Al12 phase as the temperature increases.The interfacial layers are continuously distributed along the rolling direction(RD) and transverse direction(TD).The tensile strength and elongation of Mg/Al laminated composites along RD and TD increase at first and then decrease with the increase of annealing temperature.The optimal mechanical performance is obtained when the annealing temperature is 300℃.The tensile strength along the RD and TD are 242 MPa and 247 MPa,respectively,and the elongation is more than 14%,which is obviously higher than that of the plates without annealing.The research results provide experimental reference for preparing high quality Mg/Al laminated composites based on LSDR principle.

       

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