激光熔覆Ni基复合涂层的微观组织与性能研究

    Study on Microstructure and Properties of Laser Cladding Ni-based Composite Coating

    • 摘要: 为了探究激光熔覆Ni基复合涂层的微观组织与性能,采用激光熔覆技术在316L不锈钢表面制备Ni60/WC复合涂层,利用光学显微镜、X射线衍射仪等研究了涂层的形貌和相结构;采用显微硬度计和电化学工作站等设备表征了涂层的硬度分布和耐腐蚀性能。结果表明,涂层与基材结合良好,稀释率为28.6%;涂层中生成了Cr0.19Fe0.7Ni0.11、Ni2.9Cr0.7Fe0.36和FeNi3等金属化合物以及CoCx等碳化物。涂层的硬度为316L不锈钢的3.5倍,耐腐蚀性也得到了显著提高,碳化物增强相的形成是涂层硬度、耐腐蚀性提高的主要原因,此研究结果对激光熔覆添加WC的Ni60制备有一定指导作用。

       

      Abstract: In order to explore the influence of the microstructure and performance of laser coated Ni-based composite coating, Ni60/WC composite coating was prepared on 316L stainless steel surface by laser cladding technique. The morphology and phase structure of the coating were studied by optical microscope and X-ray diffraction. The hardness distribution and corrosion resistance of the coating were characterized by microhardness tester and electrochemical workstation. The results show that the coating is well bonded with the substrate, and the dilution rate is 28.6%. Metal compounds such as Cr0.19Fe0.7Ni0.11, Ni2.9Cr0.7Fe0.36and FeNi3, and carbides such as CoCxare formed in the coating. The hardness of the coating is 3.5 times than that of 316L stainless steel, and the corrosion resistance of the coating is also significantly improved. The formation of carbide reinforcing phase is the main reason for the improvement of the hardness and corrosion resistance of the coating. The results can guide the preparation of Ni60 with WC.

       

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