降镍增氮对18Cr-5Ni不锈钢组织及热塑性的影响

    Effect of Reducing Nickel and Increasing Nitrogen on Microstructure and Thermoplasticity of 18Cr-5Ni Stainless Steel

    • 摘要: 采用Thermal-Calc2020a热力学软件对18Cr-5Ni不锈钢进行热力学平衡计算,采用Gleeble-1500D热模拟机对加入0.24wt% N的18Cr-5Ni不锈钢进行热压缩测试,测定变形温度1273~1473 K区间和应变速率为0.01~10 s-1时热压缩的应力-应变曲线,采用Zener-Hollomon参数法构建高温塑性变形的本构方程,对高温压缩变形金相组织进行了研究。结果表明:氮促进18Cr-5Ni不锈钢形成单一奥氏体组织;氮对试验钢有强化作用,应力-应变曲线中存在动态再结晶特征。加氮后热变形激活能为475.24 kJ/mol;加氮促进碳氮化物析出,氮推迟了该钢的动态再结晶过程,在高温和低应变速率下,动态再结晶容易发生。

       

      Abstract: Thermodynamic balance calculation of 18Cr-5Ni stainless steel was performed by using Thermal-Calc2020a thermodynamic software,and hot compression test of 18Cr-5Ni stainless steel added with 0.24wt% N was tested by Gleeble-1500D thermal simulator. The stress-strain curves of hot compression in the range of deformation temperature of 1273-1473 K and strain rate of 0.01-10 s-1 were measured. The constitutive equation of high temperature plastic deformation was constructed by the Zener-Hollomon parameter method.The metallographic structure of hot compression deformation was studied. The results show that nitrogen promotes the formation of single austenite structure of 18Cr-5Ni stainless steel; nitrogen has a strengthening effect on the tested steel.Dynamic recrystallization characteristics exist in the stress-strain curves.The activation energy of thermal deformation after adding nitrogen is 475.24 kJ/mol. Nitrogen addition promotes carbon nitride precipitation, and nitrogen delays the dynamic recrystallization process of the steel.Dynamic recrystallization is easy to occur at high temperature and low strain rate.

       

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